2H-CuSco? Prepared by Low-Temperature Hydrothermal Methods and Post-Annealing Effects on Optical and Photoelectrochemical Properties
By Draskovic, Thomas I.; Yu, Mingzhe & Wu, Yiying
Published in Inorganic Chemistry
NULL
2015
Abstract
The delafossite structured CuSco? is a p-type, wide band gap oxide that has been shown to support significant oxygen intercalation, leading to darkened color and increased conductivity. Control of this oxidation proves difficult by the conventional high-temperature solid-state syntheses. In addition, a pure hexagonal (2H) or rhombohedral (3R) polytype of CuSco? requires careful control of synthetic parameters or intentional doping. Lower-temperature hydrothermal syntheses have thus far led to only a mixed 2H/3R product. Herein, control of hydrothermal conditions with the consideration of copper and scandi
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