Titania nanotubes from weak organic acid electrolyte: Fabrication, characterization and oxide film properties
By Balakrishnan Munirathinam and Lakshman Neelakantan
Published in Materials Science and Engineering: C
NULL
2015
Abstract
In this study, TiO2 nanotubes were fabricated using anodic oxidation in fluoride containing weak organic acid for different durations (0.5 h, 1 h, 2 h and 3 h). Scanning electron microscope (SEM) micrographs reveal that the morphology of titanium oxide varies with anodization time. Raman spectroscopy and X-ray diffraction (XRD) results indicate that the as-formed oxide nanotubes were amorphous in nature, yet transform into crystalline phases (anatase and rutile) upon annealing at 600
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