Ligand-Assisted Metal-Centered Electrocatalytic Hydrogen Evolution upon Reduction of a Bis(thiosemicarbazonato)Ni(II) Complex
By Jain, Rahul; Mamun, Abdullah Al; Buchanan, Robert M.; Kozlowski, Pawel M.; Grapperhaus, Craig A.
Published in Inorganic Chemistry
2018
Abstract
In this study, we report the electrocatalytic behavior of the neutral, monomeric Ni(II) complex of diacetyl-bis(N-4-methyl-3-thiosemicarbazonato), NiL1, for ligand-assisted metal-centered hydrogen evolution in acetonitrile (ACN) and dimethylformamide (DMF). Using foot-of-the-wave analysis (FOWA), NiL1 displays a maximum turnover frequency (TOF) of 4200 and 1200 s
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