Quantification of CO2 from electrochemical oxidation reactions with a strategy based on transmission infrared spectroscopy
By Karthikeyan, Annamalai; Martindale, Chad & Martin, Steve W.
Published in Electrochimica Acta
NULL
2002
Abstract
The use of a micro-volume infrared transmission flow cell for quantitative determinations of CO2 dissolved in solutions following electrochemical oxidation reactions is described. Results are compared with previous in situ infrared measurements as a step toward evaluating the performance of infrared spectroelectrochemical cells under conditions where non-ideal optical effects can become important. The electrochemical oxidation of formic acid on platinum is investigated as a model.
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