Electrochemical, spectroelectrochemical and electrocatalytic properties of newly synthesized phthalocyanine compounds with 1,1?-thiobis(2-naphthol) groups
By Arucu, Sevin
Published in Journal of Molecular Structure
2019
Abstract
In this work, the synthesis and characterization of new phthalocyanine compounds containing 1,1?-thiobis(2-napthol) units have been reported. The metal-free phthalocyanine, H2Pc 3 was synthesized by the cyclotetramerization of dinitrile derivative 2 in dry n-pentanol by a classical method. Metal phthalocyanines complexes, ZnPc 4 and CoPc 5 were prepared by the reaction of 2 with the corresponding anhydrous metal salts in n-pentanol and DBU. The structures of the original compounds were identified by using elemental analysis, 1H NMR, 13C NMR, IR, mass and UV
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